Analysis of Blast Furnace Slags by Laser-Ablation Optical Emission Spectrometry with Inductively Coupled Plasma

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Authors	PISTEKOVA Marie OTRUBA Vítězslav KANICKÝ Viktor
Year of publication	2010
Type	Article in Periodical
Magazine / Source	CHEMICKÉ LISTY
MU Faculty or unit	Faculty of Science
Citation
Web	http://www.chemicke-listy.cz/ojs3/index.php/chemicke-listy/article/view/1284
Keywords	WASTE-WATER TREATMENT; LA-ICP-MS; MASS-SPECTROMETRY; SILICATE ROCKS; MINOR ELEMENTS; REMOVAL; SOLIDS; CEMENT
Description	Laser ablation (LA) has been used as a direct solid-sample introduction technique in analysis of blast-furnace slags by inductively coupled plasma optical emission spectrometry (ICP-OES). Pressed pellets containing slag and a binder, powdered Ag or a LiBO(2) - Ag mixture and an internal standard are used. The LiBO(2) mixture was found optimal. A linear calibration curve was obtained up to specified contents of metal oxides. As follows from comparison of different methods of analysis of blast-furnace slags, using reference materials and real samples, the LA ICP-OES is a suitable method for the purpose.
Related projects:	Study and application of plasma chemical reactions in non-isothermic low temperature plasma and its interaction with solid surface